The research considers conducting orthogonal experiment (OT) as one of the stages in developing a new discrete element method (DEM) parameters calibration approach. The measured responses in experiment are the parameters obtained by DEM animation processing using machine vision system (MVS). The variable factors in experiment are DEM parameters. A brief overview of an existing calibration approaches given in the article. The choice of OT as a design of experiment tool among other mathematical tools discussed. Experiments conducted using specially developed rig where bulk material's flow captured as DEM animation. DEM animation converted to video and then processed using MVS that allow register the values of such parameters as angle of repose or expiration time (measured responses). The results of the OT show that it is possible to identify four measured responses with the most valuable correlation coefficient. DEM parameters with the biggest influence on the measured responses identified for each of the obtained regression. Obtained results are useful in learning or iterative algorithms development for DEM parameters calibration.

The relevance of the research is due to the need to stabilize the composition of the melting products of copper-nickel sulfide raw materials in the Vanyukov furnace. The goal of this research is to identify the most suitable methods for the aggregation of the real time data for the development of a mathematical model for control of the technological process of melting copper-nickel sulfide raw materials in the Vanyukov furnace. Statistical methods of analyzing the historical data of the real technological object and the correlation analysis of process parameters are described. Factors that exert the greatest influence on the main output parameter (copper content in matte) and ensure the physical-chemical transformations are revealed. An approach to the processing of the real time data for the development of a mathematical model for control of the melting process is proposed. The stages of processing the real time information are considered. The adopted methodology for the aggregation of data suitable for the development of a control model for the technological process of melting copper-nickel sulfide raw materials in the Vanyukov furnace allows us to interpret the obtained results for their further practical application.

A lot of researchers are developing new DEM parameters calibration approaches based on an experiment plan or the use of learning algorithms. This research is aimed at improving iterative algorithms frequently used for calibration. The big time consumption as a main problem of iterative algorithms is questioned. It is proposed to use Random forest algorithm to determine DEM parameters impact on the measured bulk responses. Measured responses are the parameters obtained by image processing using a technical vision system. As a result of 200 experiments processing, DEM parameters impact values on each bulk response were generated and presented as histograms. Obtained results were interpreted on the basis of the bulk material behavior and its physical properties. There is a discussion on the possibility of developing a universal DEM parameters calibration method based on the iterative algorithm.